The thermal decomposition of monohydrated ammonium oxotris (oxalate) niobate
The thermal decomposition in argon of the monohydrated ammonium tris(oxalate)niobate, (NH4)3NbO(C2O4)3.H 2O, has been studied by TG/DTG, DTA, DSC, IR absorption and XRD. The material decomposes stepwise by the release of CO, CO2, NH3 and water. The atomic structure of the complex initially becomes a...
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ri-123456789-328122021-08-20T14:46:12Z The thermal decomposition of monohydrated ammonium oxotris (oxalate) niobate Medeiros, F. F. P. Moura, Maria de Fátima Vitória de Silva, A. G. P. da Souza, Carlson Pereira de Gomes, K. K. P. Gomes, Uílame Umbelino Gomes Thermal decomposition Thermal analysis Infrared Niobium complex The thermal decomposition in argon of the monohydrated ammonium tris(oxalate)niobate, (NH4)3NbO(C2O4)3.H 2O, has been studied by TG/DTG, DTA, DSC, IR absorption and XRD. The material decomposes stepwise by the release of CO, CO2, NH3 and water. The atomic structure of the complex initially becomes amorphous and then crystallizes twice in the form of orthorhombic and monoclinic niobium pentoxide 2021-07-05T18:46:14Z 2021-07-05T18:46:14Z 2006-12 article MEDEIROS, Francisca de Fatima Pegado de; MOURA, M. F. V.; SILVA, Angelus Giusepe Pereira da; SOUZA, Carlson Pereira de; GOMES, Kalyanne Keyle Pereira; GOMES, Uílame Umbelino. The thermal decomposition of monohydrated ammonium oxotris (oxalate) niobate. Brazilian Journal of Chemical Engineering, v. 23, p. 531-538, 2006. Disponível em: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0104-66322006000400011. Acesso em: 23 abr. 2021. https://doi.org/10.1590/S0104-66322006000400011 https://repositorio.ufrn.br/handle/123456789/32812 10.1590/S0104-66322006000400011 en Attribution-NonCommercial 3.0 Brazil http://creativecommons.org/licenses/by-nc/3.0/br/ application/pdf Brazilian Journal of Chemical Engineering |
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Thermal decomposition Thermal analysis Infrared Niobium complex |
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Thermal decomposition Thermal analysis Infrared Niobium complex Medeiros, F. F. P. Moura, Maria de Fátima Vitória de Silva, A. G. P. da Souza, Carlson Pereira de Gomes, K. K. P. Gomes, Uílame Umbelino Gomes The thermal decomposition of monohydrated ammonium oxotris (oxalate) niobate |
description |
The thermal decomposition in argon of the monohydrated ammonium tris(oxalate)niobate, (NH4)3NbO(C2O4)3.H 2O, has been studied by TG/DTG, DTA, DSC, IR absorption and XRD. The material decomposes stepwise by the release of CO, CO2, NH3 and water. The atomic structure of the complex initially becomes amorphous and then crystallizes twice in the form of orthorhombic and monoclinic niobium pentoxide |
format |
article |
author |
Medeiros, F. F. P. Moura, Maria de Fátima Vitória de Silva, A. G. P. da Souza, Carlson Pereira de Gomes, K. K. P. Gomes, Uílame Umbelino Gomes |
author_facet |
Medeiros, F. F. P. Moura, Maria de Fátima Vitória de Silva, A. G. P. da Souza, Carlson Pereira de Gomes, K. K. P. Gomes, Uílame Umbelino Gomes |
author_sort |
Medeiros, F. F. P. |
title |
The thermal decomposition of monohydrated ammonium oxotris (oxalate) niobate |
title_short |
The thermal decomposition of monohydrated ammonium oxotris (oxalate) niobate |
title_full |
The thermal decomposition of monohydrated ammonium oxotris (oxalate) niobate |
title_fullStr |
The thermal decomposition of monohydrated ammonium oxotris (oxalate) niobate |
title_full_unstemmed |
The thermal decomposition of monohydrated ammonium oxotris (oxalate) niobate |
title_sort |
thermal decomposition of monohydrated ammonium oxotris (oxalate) niobate |
publisher |
Brazilian Journal of Chemical Engineering |
publishDate |
2021 |
url |
https://repositorio.ufrn.br/handle/123456789/32812 |
work_keys_str_mv |
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