Anacardium occidentale L. leaves extraction via SFE: Global yields, extraction kinetics, mathematical modeling and economic evaluation
The purpose of this work was to obtain extracts from Anacardium occidentale leaves using supercritical fluid extraction (SFE). The use of ethanol and isopropyl alcohol as co-solvents was evaluated. Mass transfer kinetics experiments were performed, and overall extraction curves were modeled. SFE pro...
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ri-123456789-325382021-05-18T23:58:36Z Anacardium occidentale L. leaves extraction via SFE: Global yields, extraction kinetics, mathematical modeling and economic evaluation Leitão, Nayane Carla Márcia Cavalcanti de Sá Prado, Helena Carvalho do Veggi, Priscilla Carvalho Meireles, Maria Angela Almeida Courtial, Camila Gambini Pereira Anacardium occidentale Functional compounds Supercritical fluid extraction Kinetic parameters Economic evaluation The purpose of this work was to obtain extracts from Anacardium occidentale leaves using supercritical fluid extraction (SFE). The use of ethanol and isopropyl alcohol as co-solvents was evaluated. Mass transfer kinetics experiments were performed, and overall extraction curves were modeled. SFE process was compared with different low pressure solvent extraction processes in terms of global yield and the composition of the extract. The techniques used as low pressure solvent extraction processes were: Soxhlet extraction, agitated bed extraction, ultrasound assisted extraction using ethanol as the solvent and hydrodistillation. The extracts were analyzed by thin layer chromatography (TLC) using different eluents. Finally, the economic evaluation was conducted using the software SuperPro designer 6.0® to simulate the process and to estimate the cost of manufacturing (COM) of SFE extracts. The results indicated the presence of essential oils, lavonoids and antioxidant compounds in all the extracts. The higher yield of extract was obtained with the ultrasound assisted extraction. However, the samples with more functional compounds were verified in the SFE extracts and the extracts showed low COM. The model that best described the overall extraction curves for the SFE process was the Sovová model, which showed minimum values for the sum of the squares of the residues 2021-05-18T23:58:35Z 2021-05-18T23:58:35Z 2013-03-22 article LEITÃO, N.C.M.C.S.; Prado, G.H.C.; VEGGI, P.C.; MEIRELES, M.A.A.; Pereira, C.G.. Anacardium occidentale L leaves extraction via SFE: global yields, extraction kinetics, mathematical modeling and economic evaluation. The Journal of Supercritical Fluids, v. 78, p. 1, 2013. Disponível em: https://www.sciencedirect.com/science/article/abs/pii/S0896844613001228?via%3Dihub. Acesso em: 06 abr. 2021. https://doi.org/10.1016/j.supflu.2013.03.024 0896-8446 https://repositorio.ufrn.br/handle/123456789/32538 10.1016/j.supflu.2013.03.024 en Attribution 3.0 Brazil http://creativecommons.org/licenses/by/3.0/br/ application/pdf Elsevier |
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Anacardium occidentale Functional compounds Supercritical fluid extraction Kinetic parameters Economic evaluation |
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Anacardium occidentale Functional compounds Supercritical fluid extraction Kinetic parameters Economic evaluation Leitão, Nayane Carla Márcia Cavalcanti de Sá Prado, Helena Carvalho do Veggi, Priscilla Carvalho Meireles, Maria Angela Almeida Courtial, Camila Gambini Pereira Anacardium occidentale L. leaves extraction via SFE: Global yields, extraction kinetics, mathematical modeling and economic evaluation |
description |
The purpose of this work was to obtain extracts from Anacardium occidentale leaves using supercritical fluid extraction (SFE). The use of ethanol and isopropyl alcohol as co-solvents was evaluated. Mass transfer kinetics experiments were performed, and overall extraction curves were modeled. SFE process was compared with different low pressure solvent extraction processes in terms of global yield and the composition of the extract. The techniques used as low pressure solvent extraction processes were: Soxhlet extraction, agitated bed extraction, ultrasound assisted extraction using ethanol as the solvent and hydrodistillation. The extracts were analyzed by thin layer chromatography (TLC) using different eluents. Finally, the economic evaluation was conducted using the software SuperPro designer 6.0® to simulate the process and to estimate the cost of manufacturing (COM) of SFE extracts. The results indicated the presence of essential oils,
lavonoids and antioxidant compounds in all the extracts. The higher yield of extract was obtained with the ultrasound assisted extraction. However, the samples with more functional compounds were verified in the SFE extracts and the extracts showed low COM. The model that best described the overall extraction curves for the SFE process was the Sovová model, which showed minimum values for the sum of the squares of the residues |
format |
article |
author |
Leitão, Nayane Carla Márcia Cavalcanti de Sá Prado, Helena Carvalho do Veggi, Priscilla Carvalho Meireles, Maria Angela Almeida Courtial, Camila Gambini Pereira |
author_facet |
Leitão, Nayane Carla Márcia Cavalcanti de Sá Prado, Helena Carvalho do Veggi, Priscilla Carvalho Meireles, Maria Angela Almeida Courtial, Camila Gambini Pereira |
author_sort |
Leitão, Nayane Carla Márcia Cavalcanti de Sá |
title |
Anacardium occidentale L. leaves extraction via SFE: Global yields, extraction kinetics, mathematical modeling and economic evaluation |
title_short |
Anacardium occidentale L. leaves extraction via SFE: Global yields, extraction kinetics, mathematical modeling and economic evaluation |
title_full |
Anacardium occidentale L. leaves extraction via SFE: Global yields, extraction kinetics, mathematical modeling and economic evaluation |
title_fullStr |
Anacardium occidentale L. leaves extraction via SFE: Global yields, extraction kinetics, mathematical modeling and economic evaluation |
title_full_unstemmed |
Anacardium occidentale L. leaves extraction via SFE: Global yields, extraction kinetics, mathematical modeling and economic evaluation |
title_sort |
anacardium occidentale l. leaves extraction via sfe: global yields, extraction kinetics, mathematical modeling and economic evaluation |
publisher |
Elsevier |
publishDate |
2021 |
url |
https://repositorio.ufrn.br/handle/123456789/32538 |
work_keys_str_mv |
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