Structural and morphological characterization of rare earth modified lead titanate
Rare earth modified lead titanate powders Pb1-xRExTiO3 (REPT), x = 0.01, 0.05, 0.07 and RE = Yb, Y, were prepared by the Pechini method. The materials were calcined under flowing oxygen at different temperatures from 300 to 700 ºC. Nanostructured REPT were investigated using X-ray diffraction, scann...
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ri-123456789-322592021-04-19T20:16:04Z Structural and morphological characterization of rare earth modified lead titanate Caracterização estrutural e morfológica de titanatos de chumbo modificados por terras raras Lemos, F. C. D. Melo, Dulce Maria de Araújo Lima, P. S. de Paskocimas, Carlos Alberto Silva, Elson Longo da Silva, J. E. C. da PbTiO3 Terra Rara Perovsquita Método Pechini. Rare earth modified lead titanate powders Pb1-xRExTiO3 (REPT), x = 0.01, 0.05, 0.07 and RE = Yb, Y, were prepared by the Pechini method. The materials were calcined under flowing oxygen at different temperatures from 300 to 700 ºC. Nanostructured REPT were investigated using X-ray diffraction, scanning electron microscopy and surface area analysis (BET). The results suggest that the modifier cation incorporated into the system has notable influence in the microstructure and a notable decrease in the crystallite sizes Pós de titanatos de chumbo modificados por terras raras, Pb1-xRExTiO3 (REPT), x = 0,01, 0,05, 0.07 e RE = Yb, Y, foram preparados pelo método Pechini. Os materiais foram calcinados sob fluxo de oxigênio a diferentes temperatures de 300 a 700 ºC. Os REPT nanoestruturados obtidos foram investigados utilizando as técnicas de difração de raios X (DRX), microscopia eletrônica de varredura (MEV) e análise de area superficial (BET). Os resultados sugerem que o cátion dopante incorporado ao sistema tem notável influência na microestrutura e na diminuição dos tamanhos dos cristalitos 2021-04-16T18:04:37Z 2021-04-16T18:04:37Z 2007-10 article LEMOS, F. C. D.; MELO, D. M. A.; LIMA, P. S. de; PASKOCIMAS, C. A.; LONGO, E.; SILVA, J. E.C. da. Structural and morphological characterization of rare earth modified lead titanate. Cerâmica, [S.L.], v. 53, n. 328, p. 422-447, dez. 2007. Disponível em: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0366-69132007000400017&lng=en&tlng=en. Acesso em: 12 mar. 2021. http://dx.doi.org/10.1590/s0366-69132007000400017. 10.1590/s0366-69132007000400017. 0366-6913 https://repositorio.ufrn.br/handle/123456789/32259 en Attribution-NonCommercial 3.0 Brazil http://creativecommons.org/licenses/by-nc/3.0/br/ application/pdf ABCERAM |
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PbTiO3 Terra Rara Perovsquita Método Pechini. |
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PbTiO3 Terra Rara Perovsquita Método Pechini. Lemos, F. C. D. Melo, Dulce Maria de Araújo Lima, P. S. de Paskocimas, Carlos Alberto Silva, Elson Longo da Silva, J. E. C. da Structural and morphological characterization of rare earth modified lead titanate |
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Rare earth modified lead titanate powders Pb1-xRExTiO3 (REPT), x = 0.01, 0.05, 0.07 and RE = Yb, Y, were prepared by the Pechini method. The materials were calcined under flowing oxygen at different temperatures from 300 to 700 ºC. Nanostructured REPT were investigated using X-ray diffraction, scanning electron microscopy and surface area analysis (BET). The results suggest that the modifier cation incorporated into the system has notable influence in the microstructure and a notable decrease in the crystallite sizes |
format |
article |
author |
Lemos, F. C. D. Melo, Dulce Maria de Araújo Lima, P. S. de Paskocimas, Carlos Alberto Silva, Elson Longo da Silva, J. E. C. da |
author_facet |
Lemos, F. C. D. Melo, Dulce Maria de Araújo Lima, P. S. de Paskocimas, Carlos Alberto Silva, Elson Longo da Silva, J. E. C. da |
author_sort |
Lemos, F. C. D. |
title |
Structural and morphological characterization of rare earth modified lead titanate |
title_short |
Structural and morphological characterization of rare earth modified lead titanate |
title_full |
Structural and morphological characterization of rare earth modified lead titanate |
title_fullStr |
Structural and morphological characterization of rare earth modified lead titanate |
title_full_unstemmed |
Structural and morphological characterization of rare earth modified lead titanate |
title_sort |
structural and morphological characterization of rare earth modified lead titanate |
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ABCERAM |
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2021 |
url |
https://repositorio.ufrn.br/handle/123456789/32259 |
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