Structural characterization of phase transition of Al2O3 nanopowders obtained by polymeric precursor method
Nanocrystalline Al2O3powders have been synthesized by the polymeric precursor method. A study of the evolution of crystalline phases of obtained powders was accomplished through X-ray diffraction, micro-Raman spectroscopy and refinement of the structures through the Rietveld method. The results obta...
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Principais autores: | , , , , , , |
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Formato: | article |
Idioma: | English |
Publicado em: |
Elsevier
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Endereço do item: | https://repositorio.ufrn.br/handle/123456789/32253 |
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Resumo: | Nanocrystalline Al2O3powders have been synthesized by the polymeric precursor method. A study of the evolution of crystalline phases of obtained powders was accomplished through X-ray diffraction, micro-Raman spectroscopy and refinement of the structures through the Rietveld method. The results obtained allow the identification of three steps on the -Al2O3 to -Al2O3 phase transition. The single-phase -Al2O3 powder
was obtained after heat-treatment at 1050 ◦ C for 2 h. A study of the morphology of the particles was accomplished through measures of crystallite size, specific surface area and transmission electronic microscopy. The particle size is closely related to -Al2O3 to -Al2O3 phase transition |
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